dihydrocuscohydrine

Base Information

Chemical Name:dihydrocuscohydrine
CAS No.:468732-35-6
Molecular Formula:C₁₃H₂₆N₂O
Molecular Weight:226.362
Hs Code.:

Synonyms:

Suppliers and Price of dihydrocuscohydrine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dihydrocuscohydrine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dihydrocuscohydrine

There total 8 articles about dihydrocuscohydrine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 466645-84-1
C₁₉H₄₀N₂OSi

: 468732-35-6,80408-57-7
dihydrocuscohydrine

Guidance literature:: With hydrogenchloride; In ethanol;
DOI:10.1021/jo025666l

Reference yield:

: 134734-52-4
(1R,4S,6S)-4-acetoxy-6-[(tert-butyldimethylsilyl)oxy]-2-cyclohepten-1-ol

: 468732-35-6,80408-57-7
dihydrocuscohydrine

Guidance literature:: Multi-step reaction with 8 steps

1.1: 82 percent / diisopropylazodicarboxylate; PPh₃ / tetrahydrofuran / 18 h / 20 °C

2.1: 95 percent / KCN / methanol / 18 h / 20 °C

3.1: 85 percent / mesyl chloride; pyridine / 18 h / 20 °C

4.1: 86 percent / K₂CO₃ / acetonitrile / 18 h / 70 °C

5.1: K₂CO₃; PhSH / dimethylformamide / 0.5 h / 70 °C

5.2: 82 percent / dimethylformamide / 2 h / 20 °C

6.1: [Ru(PCy₃)2Cl₂=CHPh] / CH₂Cl₂ / 36 h / Heating

6.2: 72 percent / H₂ / 10percent Pd/C / ethanol / 20 °C

7.1: 92 percent / LiAlH₄ / diethyl ether / 0.75 h / 20 °C

8.1: 89 percent / conc. HCl / ethanol

With pyridine; hydrogenchloride; potassium cyanide; lithium aluminium tetrahydride; Grubbs catalyst first generation; di-isopropyl azodicarboxylate; potassium carbonate; methanesulfonyl chloride; thiophenol; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1.1: Mitsunobu reaction;
DOI:10.1021/jo025666l

Reference yield:

: 466645-80-7
N-allyl-N-[6-(tert-butyl-dimethyl-silanyloxy)-4-chloro-cyclohept-2-enyl]-4-nitro-benzenesulfonamide

: 468732-35-6,80408-57-7
dihydrocuscohydrine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 86 percent / K₂CO₃ / acetonitrile / 18 h / 70 °C

2.1: K₂CO₃; PhSH / dimethylformamide / 0.5 h / 70 °C

2.2: 82 percent / dimethylformamide / 2 h / 20 °C

3.1: [Ru(PCy₃)2Cl₂=CHPh] / CH₂Cl₂ / 36 h / Heating

3.2: 72 percent / H₂ / 10percent Pd/C / ethanol / 20 °C

4.1: 92 percent / LiAlH₄ / diethyl ether / 0.75 h / 20 °C

5.1: 89 percent / conc. HCl / ethanol

With hydrogenchloride; lithium aluminium tetrahydride; Grubbs catalyst first generation; potassium carbonate; thiophenol; In diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo025666l