Dichlorodiphenylethylene

Base Information

• Chemical Name: Dichlorodiphenylethylene
• CAS No.: 13700-82-8
• Molecular Formula: C14H10Cl2
• Molecular Weight: 249.139
• Hs Code.: 2903999090
• European Community (EC) Number: 660-652-2
• DSSTox Substance ID: DTXSID20871815
• Mol file: 13700-82-8.mol

Synonyms:13700-82-8;dichlorodiphenylethylene;DTXSID20871815;1,2-Dichloro-1,2-diphenylethene;1,1'-[(E)-1,2-Dichloroethene-1,2-diyl]dibenzene

Chemical Property of Dichlorodiphenylethylene

Chemical Property:

• Melting Point: 193-194 °C
• Boiling Point: 104-106 °C(Press: 6.1 Torr)
• PSA: 0.00000
• Density: 1.232±0.06 g/cm3(Predicted)
• LogP: 4.99000
• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 248.0159557
• Heavy Atom Count: 16
• Complexity: 220

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=C(C2=CC=CC=C2)Cl)Cl

Technology Process of Dichlorodiphenylethylene

There total 10 articles about Dichlorodiphenylethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

diphenyl acetylene (501-65-5) → 1,2-dichloro-1,2-diphenylethylene (13700-82-8)

Guidance literature:

With hydrogenchloride; iodosylbenzene; for 0.0833333h;

DOI:10.1016/S0040-4020(98)00844-8

Reference yield: 48.0%

cyclohexane (110-82-7,25012-93-5) + 3-Chlor-3-phenyl-1,2-diaziridin (74670-99-8) → 1,2-bis[chloro(phenyl)methylidene]hydrazone (729-44-2,116377-04-9) + (chloro-cyclohexyl-methyl)benzene (28047-23-6) + 1,2-dichloro-1,2-diphenylethylene (13700-82-8)

Guidance literature:

In benzene; at 23 ℃; Kinetics; Irradiation; activation parameters was determined;

DOI:10.1016/S0040-4039(98)02196-0

Reference yield: 48.0%

3-Chlor-3-phenyl-1,2-diaziridin (74670-99-8) + paracetaldehyde (123-63-7) → 1,2-bis[chloro(phenyl)methylidene]hydrazone (729-44-2,116377-04-9) + 1,2-dichloro-1,2-diphenylethylene (13700-82-8) + 2-(chloro-phenyl-methyl)-2,4,6-trimethyl-[1,3,5]trioxane

Guidance literature:

In benzene; at 23 ℃; Kinetics; Irradiation; activation parameters was determined;

DOI:10.1016/S0040-4039(98)02196-0

upstream raw materials:

diphenyl acetylene

cyclohexane

3-Chlor-3-phenyl-1,2-diaziridin

paracetaldehyde

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