4,6-bis(diphenylphosphanyl)dibenzofuran(tri-p-tolylphosphane)ruthenium dichloride

Base Information

Chemical Name:4,6-bis(diphenylphosphanyl)dibenzofuran(tri-p-tolylphosphane)ruthenium dichloride
CAS No.:195449-00-4
Molecular Formula:C₅₇H₄₇Cl₂OP₃Ru
Molecular Weight:1012.9
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Chemical Property of 4,6-bis(diphenylphosphanyl)dibenzofuran(tri-p-tolylphosphane)ruthenium dichloride

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Technology Process of 4,6-bis(diphenylphosphanyl)dibenzofuran(tri-p-tolylphosphane)ruthenium dichloride

There total 1 articles about 4,6-bis(diphenylphosphanyl)dibenzofuran(tri-p-tolylphosphane)ruthenium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 20759-14-2,14898-67-0
ruthenium(III) chloride hydrate

: 133850-81-4
4,6-bis(diphenylphosphanyl)dibenzofuran

: 1038-95-5,218281-19-7
Tri(p-tolyl)phosphine

: 195449-00-4
4,6-bis(diphenylphosphanyl)dibenzofuran(tri-p-tolylphosphane)ruthenium dichloride

Guidance literature:: In ethanol; (argon); refluxing RuCl3*H2O in EtOH for 40 h, addn. of the two ligands in EtOH, further reflux (10 h); filtration, washing (EtOH), drying (vac.); elem. anal.;