Cp*2ZrCH₂CCHCMeCHCMeCSiHMes

Base Information

• Chemical Name: Cp*2ZrCH₂CCHCMeCHCMeCSiHMes
• CAS No.: 117940-88-2
• Molecular Formula: C₃₈H₅₂SiZr
• Molecular Weight: 628.14
• Mol file: 117940-88-2.mol

Synonyms:

Chemical Property of Cp*2ZrCH₂CCHCMeCHCMeCSiHMes

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Cp*2ZrCH₂CCHCMeCHCMeCSiHMes

There total 2 articles about Cp*2ZrCH₂CCHCMeCHCMeCSiHMes which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

bis(pentamethylcyclopentadienyl)zirconium(IV) dichloride (54039-38-2) + (THF)2LiSiHMes2 → Cp*2ZrCH2CCHCMeCHCMeCSiHMes (117940-88-2)

Guidance literature:

In toluene; byproducts: ((CH3)3C6H2)2SiH2; soln. of Zr-compd. stirred at ambient temp. for 5h, volatiles removed, residue taken up in warm toluene, filtered; exclusion of air and moisture; solvent removed, resulting solid slurried in Et2O, filtration, washed (diethyl ether), dried (vac.);

DOI:10.1021/om00104a009

Reference yield:

(THF)2LiSiHMes2 + Cp*2Zr(SiHMes)2Cl (117940-83-7) → Cp*2ZrCH2CCHCMeCHCMeCSiHMes (117940-88-2)

Guidance literature:

In not given;

DOI:10.1021/om00104a009

upstream raw materials:

Cp*2Zr(SiHMes)2Cl

bis(pentamethylcyclopentadienyl)zirconium(IV) dichloride