Cp*2Zr(SiHMes)2Cl

Base Information

• Chemical Name: Cp*2Zr(SiHMes)2Cl
• CAS No.: 117940-83-7
• Molecular Formula: C₃₈H₅₃ClSiZr
• Molecular Weight: 664.601
• Mol file: 117940-83-7.mol

Synonyms:

Chemical Property of Cp*2Zr(SiHMes)2Cl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Cp*2Zr(SiHMes)2Cl

There total 1 articles about Cp*2Zr(SiHMes)2Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

hydrogenchloride (7647-01-0,15364-23-5) + Cp*2Zr(SiHMes2)Me (117940-82-6) → Cp*2Zr(SiHMes)2Cl (117940-83-7)

Guidance literature:

In toluene; byproducts: CH4; addn. of HCl to a rapidly stirred soln. of Zr-compd. at -78°C, evolution of gas, after 30 min. soln. allowed to warm to ambinet temp.; exclusion of air and moisture; solvent removed, residue slurried in pentane, filtered, dried (vac.); elem. anal.;

DOI:10.1021/om00104a009

Reference yield:

(THF)2LiSiHMes2 + Cp*2Zr(SiHMes)2Cl (117940-83-7) → Cp*2ZrCH2CCHCMeCHCMeCSiHMes (117940-88-2)

Guidance literature:

In not given;

DOI:10.1021/om00104a009

upstream raw materials:

hydrogenchloride

Cp*2Zr(SiHMes₂)Me

Downstream raw materials:

Cp*2ZrCH₂CCHCMeCHCMeCSiHMes