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Technology Process of (CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

(CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

Base Information Edit
  • Chemical Name:(CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4
  • CAS No.:208589-74-6
  • Molecular Formula:C11H22N3Pd*C32H12BF24
  • Molecular Weight:1165.96
  • Hs Code.:
  • Mol file:208589-74-6.mol
(CH<sub>3</sub>CN)Pd(CH<sub>3</sub>)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2<sup>(1+)</sup>*B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4<sup>(1-)</sup>=CH<sub>3</sub>CNPd(CH<sub>3</sub>)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4

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Chemical Property of (CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4 Edit
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Technology Process of (CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

There total 1 articles about (CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(i-Pr-1,4-diazabutadiene)(metyl)chloropalladium(II)
350016-97-6

(i-Pr-1,4-diazabutadiene)(metyl)chloropalladium(II)

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
79060-88-1

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

acetonitrile
75-05-8,26809-02-9

acetonitrile

(CH<sub>3</sub>CN)Pd(CH<sub>3</sub>)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2<sup>(1+)</sup>*B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4<sup>(1-)</sup>=CH<sub>3</sub>CNPd(CH<sub>3</sub>)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4
208589-74-6

(CH3CN)Pd(CH3)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3CNPd(CH3)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

Guidance literature:
In dichloromethane; acetonitrile; byproducts: NaCl; (N2); addn. of a soln. of boron compd. in CH2Cl2/CH3CN (5:1) to a soln. of palladium complex in CH2Cl2/CH3CN (5:1) at -40°C, slow warmingto 0°C, stirring for 15 min; filtration through Celite, evapn., treatment with hexane at -80°C; elem. anal.;
DOI:10.1021/om000971n
upstream raw materials:

(i-Pr-1,4-diazabutadiene)(metyl)chloropalladium(II)

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

acetonitrile

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