C₁₄H₁₄⁽²⁾H₃NO

Base Information

Chemical Name:C₁₄H₁₄⁽²⁾H₃NO
CAS No.:1301714-85-1
Molecular Formula:C₁₄H₁₇NO
Molecular Weight:218.271
Hs Code.:

C<sub>14</sub>H<sub>14</sub><sup>(2)</sup>H<sub>3</sub>NO

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₄⁽²⁾H₃NO

Chemical Property:

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Technology Process of C₁₄H₁₄⁽²⁾H₃NO

There total 5 articles about C₁₄H₁₄⁽²⁾H₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1301714-84-0
N-butyl-2-(2-((trimethylsilyl)ethynyl)phenyl)acetamide

: 1301714-85-1
C₁₄H₁₄⁽²⁾H₃NO

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol; dichloromethane / 2 h / 20 °C

2: chloroform-d1; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / 12 h / 20 °C

With chloroform-d1; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium carbonate; In methanol; dichloromethane;
DOI:10.1021/jo200352j

Reference yield:

: 1301714-55-5
N-butyl-2-(2-ethynylphenyl)acetamide

: 1301714-85-1
C₁₄H₁₄⁽²⁾H₃NO

Guidance literature:: With chloroform-d1; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; at 20 ℃; for 12h;
DOI:10.1021/jo200352j

Reference yield:

: N-butyl-2-(2-iodophenyl)acetamide

: 1301714-85-1
C₁₄H₁₄⁽²⁾H₃NO

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 70 °C / Inert atmosphere

2: potassium carbonate / methanol; dichloromethane / 2 h / 20 °C

3: chloroform-d1; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / 12 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; chloroform-d1; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium carbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jo200352j