1,11-Bis--benzophenanthren

Base Information

• Chemical Name: 1,11-Bis--benzophenanthren
• CAS No.: 65796-66-9
• Molecular Formula: C₄₈H₃₀F₁₂O₂P₂
• Molecular Weight: 928.693

Synonyms:

Chemical Property of 1,11-Bis--benzophenanthren

Chemical Property:

Purity/Quality:

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Technology Process of 1,11-Bis--benzophenanthren

There total 4 articles about 1,11-Bis--benzophenanthren which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,11-bisbenzophenantrene (65796-61-4) → 1,11-Bis--benzophenanthren (65796-66-9)

Guidance literature:

With dihydrogen peroxide; In acetone;

DOI:10.1002/hlca.19770600835

Reference yield:

3-bromo-1-trifluoromethylbenzene (401-78-5) → 1,11-Bis--benzophenanthren (65796-66-9)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) Mg, Et₂O, (ii) HPO(OEt)2, (iii) aq. HCl

2: LiAlH₄ / diethyl ether / Heating

3: (i) nBuLi, hexane, THF, (ii) /BRN= 2535167/

4: aq. H₂O₂ / acetone

With lithium aluminium tetrahydride; dihydrogen peroxide; In diethyl ether; acetone;

DOI:10.1002/hlca.19770600835

Reference yield:

bis(α,α,α-trifluoro-3-tolyl)phosphine oxide (15929-44-9) → 1,11-Bis--benzophenanthren (65796-66-9)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / Heating

2: (i) nBuLi, hexane, THF, (ii) /BRN= 2535167/

3: aq. H₂O₂ / acetone

With lithium aluminium tetrahydride; dihydrogen peroxide; In diethyl ether; acetone;

DOI:10.1002/hlca.19770600835

upstream raw materials:

2,11-bisbenzophenantrene

3-bromo-1-trifluoromethylbenzene

bis(α,α,α-trifluoro-3-tolyl)phosphine oxide

bis(α,α,α-trifluoro-3-tolyl)phosphine

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