(4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III)

Base Information

• Chemical Name: (4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III)
• CAS No.: 1164142-05-5
• Molecular Formula: C₆₉H₆₁FeN₈
• Molecular Weight: 1058.14
• Mol file: 1164142-05-5.mol

Synonyms:

Chemical Property of (4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III)

There total 1 articles about (4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

5,10,15,20-tetra(2',4',6'-trimethylphenyl)porphyrinatoiron(III) chloride (136096-56-5,77439-21-5) + 4-azo-(phenylcyanamido)benzene, thallium salt → (4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III) (1164142-05-5)

Guidance literature:

In toluene; mixt. of Fe compd. and Tl salt of ligand kept under vac. for 30 min; placed under N2; dry toluene transferred; stirred for 24 h; filtered; vol. of filtrate reduced; dried n-hexane added in portion withstirring; ppt. removed by filtration; dried in air; elem. anal.;

DOI:10.1016/j.ica.2008.12.023

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + (4-azo-(phenylcyanamido)benzene)(tetramesitylporphyrinato)iron(III) (1164142-05-5) → 5,10,15,20-tetra(2',4',6'-trimethylphenyl)porphyrinatoiron(III) chloride (136096-56-5,77439-21-5)

Guidance literature:

In not given;

DOI:10.1016/j.ica.2008.12.023

upstream raw materials:

5,10,15,20-tetra(2',4',6'-trimethylphenyl)porphyrinatoiron(III) chloride

Downstream raw materials:

5,10,15,20-tetra(2',4',6'-trimethylphenyl)porphyrinatoiron(III) chloride