Technology Process of C24H28O4
There total 2 articles about C24H28O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate;
In
1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; acetonitrile;
at 120 ℃;
for 2h;
Microwave irradiation;
DOI:10.1002/chem.201101917
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C
1.2: 0 - 20 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate / 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; acetonitrile / 2 h / 120 °C / Microwave irradiation
With
tetrakis(triphenylphosphine) palladium(0); sodium hydride; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate;
In
1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/chem.201101917