tris(cyclohexylamine)molybdenum tricarbonyl

Base Information

Chemical Name:tris(cyclohexylamine)molybdenum tricarbonyl
CAS No.:21496-06-0
Molecular Formula:C₂₁H₃₉MoN₃O₃
Molecular Weight:477.499
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(cyclohexylamine)molybdenum tricarbonyl

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Technology Process of tris(cyclohexylamine)molybdenum tricarbonyl

There total 1 articles about tris(cyclohexylamine)molybdenum tricarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 21496-06-0,15083-81-5
tris(cyclohexylamine)molybdenum tricarbonyl

Guidance literature:: In tetrahydrofuran; dibutyl ether; (N2); refluxing a soln. of metal carbonyl and amine in a mixt. of d-n-butyl ether and THF for 2 h, cooling to room temp.; evapn., washing with hexane at -10°C, drying in vac.;
DOI:10.1016/S0022-328X(02)01992-7

Reference yield: 34.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 21496-06-0,15083-81-5
tris(cyclohexylamine)molybdenum tricarbonyl

: 129105-68-6,505027-56-5
(C₆H₁₁NCH₂)3Mo(CO)3

Guidance literature:: With MgSO₄; In tetrahydrofuran; (N2); addn. of aldehyde to a soln. of molybdenum complex in THF with excess MgSO4, stirring at 50°C for 3-4 h, cooling to room temp.; evapn., extn. with CH2Cl2, evapn.;
DOI:10.1016/S0022-328X(02)01992-7

Reference yield:

: 21496-06-0,15083-81-5
tris(cyclohexylamine)molybdenum tricarbonyl

: 59993-08-7
bromotris(cyclohexylamine)molybdenum tricarbonyl bromide

Guidance literature:: With bromine; In hexane; N2-atmosphere; dropwise addn. of 1 equiv. of bromine soln. to Mo-complex(room temp.); elem. anal.;
DOI:10.1016/S0020-1693(00)95609-3