perchlorate salt of tert-butyl-retinylidene imine

Base Information

• Chemical Name: perchlorate salt of tert-butyl-retinylidene imine
• CAS No.: 109719-70-2
• Molecular Formula: C₂₄H₃₇N*ClHO₄
• Molecular Weight: 440.023

Synonyms:

Chemical Property of perchlorate salt of tert-butyl-retinylidene imine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of perchlorate salt of tert-butyl-retinylidene imine

There total 1 articles about perchlorate salt of tert-butyl-retinylidene imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

all-trans-Retinal (116-31-4) + tert-butylamine (75-64-9) → perchlorate salt of tert-butyl-retinylidene imine (109719-70-2)

Guidance literature:

With perchloric acid; Multistep reaction; 1.) ether, 3 h, 2.) ether;

DOI:10.1021/ja00252a010

Reference yield:

perchlorate salt of tert-butyl-retinylidene imine (109719-70-2) → tert-Butyl-[(2E,4E,6Z,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine; compound with perchloric acid (114127-34-3) + tert-Butyl-[(2E,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine; compound with perchloric acid (114128-96-0)

Guidance literature:

In dichloromethane; at 22 ℃; Product distribution; Quantum yield; Irradiation;

DOI:10.1021/ja00218a003

upstream raw materials:

all-trans-Retinal

tert-butylamine

Downstream raw materials:

tert-Butyl-[(2E,4E,6Z,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine; compound with perchloric acid

tert-Butyl-[(2E,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine; compound with perchloric acid

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