2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

Base Information

Chemical Name:2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid
CAS No.:1353941-76-0
Molecular Formula:C₂₅H₂₇NO₄
Molecular Weight:405.494
Hs Code.:

Synonyms:

Suppliers and Price of 2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
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Technology Process of 2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

There total 5 articles about 2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 255050-65-8
6-trifluoromethanesulfonyloxy-naphthalene-1-carboxylic acid methyl ester

: 1353941-76-0
2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: iron(III)-acetylacetonate / 1-methyl-pyrrolidin-2-one; diethyl ether; tetrahydrofuran / 0.5 h / 20 °C

2: water; lithium hydroxide / tetrahydrofuran / 24 h / 40 °C / Sealed scintillation vial

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4: water; lithium hydroxide / tetrahydrofuran / 40 h / 60 °C / Sealed scintillation vial

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; iron(III)-acetylacetonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; dichloromethane;

Reference yield:

: 2437-17-4
6-hydroxy-1-naphthoic acid

: 1353941-76-0
2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: diethyl ether; tetrahydrofuran / 1.5 h / 0 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

3: iron(III)-acetylacetonate / 1-methyl-pyrrolidin-2-one; diethyl ether; tetrahydrofuran / 0.5 h / 20 °C

4: water; lithium hydroxide / tetrahydrofuran / 24 h / 40 °C / Sealed scintillation vial

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

6: water; lithium hydroxide / tetrahydrofuran / 40 h / 60 °C / Sealed scintillation vial

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; iron(III)-acetylacetonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; dichloromethane;

Reference yield:

: 90162-13-3
methyl 6-hydroxy-1-naphthoate

: 1353941-76-0
2-(3-(6-hexyl-1-naphthamido)phenoxy)acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

2: iron(III)-acetylacetonate / 1-methyl-pyrrolidin-2-one; diethyl ether; tetrahydrofuran / 0.5 h / 20 °C

3: water; lithium hydroxide / tetrahydrofuran / 24 h / 40 °C / Sealed scintillation vial

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

5: water; lithium hydroxide / tetrahydrofuran / 40 h / 60 °C / Sealed scintillation vial

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; iron(III)-acetylacetonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; dichloromethane;