1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole

Base Information

Chemical Name:1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole
CAS No.:112565-56-7
Molecular Formula:C₁₉H₁₈N₂O₂S
Molecular Weight:338.43
Hs Code.:

Synonyms:

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Chemical Property of 1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole

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Technology Process of 1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole

There total 8 articles about 1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 112565-58-9
7-Benzenesulfonyl-6-oxo-1,3,4,5,6,7-hexahydro-azocino[4,3-b]indole-2-carboxylic acid 2,2,2-trichloro-ethyl ester

: 112565-56-7
1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole

: 112565-55-6
1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indol-9 (4H)-one

Guidance literature:: With acetic acid; zinc; for 48h;
DOI:10.1039/P19870001599

Reference yield:

: 40899-71-6
1-benzenesulfonylindole

: 112565-56-7
1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole

Guidance literature:: Multi-step reaction with 7 steps

1: 72 percent / butyl-lithium / tetrahydrofuran / 1.5 h / Ambient temperature

2: 63 percent / lithium aluminium hydride / tetrahydrofuran / 12 h / Heating

3: 96 percent / acetic acid; 1,2-dimethoxy-ethane / 0.33 h / Ambient temperature

4: 53 percent / manganese dioxide / CHCl₃ / 48 h / Ambient temperature

5: 82 percent / 50percent aq. sodium hydroxide, tetrabutylammonium hydroxide / benzene / 1 h

6: 74 percent / potassium hydrogen carbonate / CHCl₃ / 8 h / Heating

7: 27 percent / zinc dust/acetic acid / 5 h

With manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; n-butyllithium; tetra(n-butyl)ammonium hydroxide; potassium hydrogencarbonate; acetic acid; zinc; In tetrahydrofuran; 1,2-dimethoxyethane; chloroform; acetic acid; benzene;
DOI:10.1039/P19870001599

Reference yield:

: 112565-48-7
2-benzyl-1,2,3,4-tetrahydroazocino<4,3-b>indol-6 (5H)-one

: 112565-56-7
1,2,3,3a,4,9-hexahydro-4-phenylsulphonylpyrrolo<1',2':1,2>pyrrolo<3,4-b>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / 50percent aq. sodium hydroxide, tetrabutylammonium hydroxide / benzene / 1 h

2: 74 percent / potassium hydrogen carbonate / CHCl₃ / 8 h / Heating

3: 27 percent / zinc dust/acetic acid / 5 h

With sodium hydroxide; tetra(n-butyl)ammonium hydroxide; potassium hydrogencarbonate; acetic acid; zinc; In chloroform; benzene;
DOI:10.1039/P19870001599