(((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D

Base Information

Chemical Name:(((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D
CAS No.:866367-31-9
Molecular Formula:C₄₁H₇₂OSi₆Sn
Molecular Weight:869.237
Hs Code.:

(((CH<sub>3</sub>)3Si)2CH)3C<sub>6</sub>H<sub>2</sub>Sn(OCH<sub>3</sub>)C<sub>13</sub>H<sub>9</sub>D

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Chemical Property of (((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D

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Technology Process of (((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D

There total 6 articles about (((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1455-13-6
deuteromethanol

: 866367-22-8
(((CH₃)3Si)2CH)3C₆H₂SnC₁₃H₉

: 866367-31-9
(((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D

Guidance literature:: With Li 2,2,6,6,-tetramethylpiperidine; compds. reacted at -78°C; detected by 1H NMR, could not be isolated as pure compd.;
DOI:10.1246/cl.2005.1088

Reference yield:

: 866367-23-9
9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

: 866367-31-9
(((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D

Guidance literature:: Multi-step reaction with 2 steps

1: tert-BuLi / not given

2: Li 2,2,6,6,-tetramethylpiperidine

With tert-BuLi; Li 2,2,6,6,-tetramethylpiperidine; In not given;
DOI:10.1246/cl.2005.1088

Reference yield:

: 866367-30-8
(((CH₃)3Si)2CH)3C₆H₂SnCl₂C₆H₄C₆H₄CH₂Br

: 866367-31-9
(((CH₃)3Si)2CH)3C₆H₂Sn(OCH₃)C₁₃H₉D

Guidance literature:: Multi-step reaction with 3 steps

1: Mg; LiAlH₄ / tetrachloromethane

2: tert-BuLi / not given

3: Li 2,2,6,6,-tetramethylpiperidine

With Mg; LiAlH₄; tert-BuLi; Li 2,2,6,6,-tetramethylpiperidine; In tetrachloromethane;
DOI:10.1246/cl.2005.1088