N¹,N¹-Diethyl-N³-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide

Base Information

• Chemical Name: N¹,N¹-Diethyl-N³-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide
• CAS No.: 86670-91-9
• Molecular Formula: BrH*C₂₅H₃₆N₄O₃S₂
• Molecular Weight: 585.63

Synonyms:

Chemical Property of N¹,N¹-Diethyl-N³-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N¹,N¹-Diethyl-N³-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide

There total 3 articles about N¹,N¹-Diethyl-N³-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-methoxy-2-nitrophenyl)-4-methylbenzenesulfonamide (3360-81-4) → N1,N1-Diethyl-N3-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide (86670-91-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 89 percent / K₂CO₃ / dimethylformamide / on steam bath

2: 76 percent / H₂ / 5percent Pd-C / ethanol; dioxane / Ambient temperature

3: 89 percent / H₂O / 1) 0 deg C, 2 h, 2) 4 deg C, several hours

4: 61 percent / diethyl ether / 3 h / Heating

With hydrogen; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)91886-1

Reference yield:

N-(2-Bromoethyl)-N-tosyl-4-methoxy-2-nitraniline (16058-88-1) → N1,N1-Diethyl-N3-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide (86670-91-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 76 percent / H₂ / 5percent Pd-C / ethanol; dioxane / Ambient temperature

2: 89 percent / H₂O / 1) 0 deg C, 2 h, 2) 4 deg C, several hours

3: 61 percent / diethyl ether / 3 h / Heating

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; ethanol; water;

DOI:10.1016/S0040-4020(01)91886-1

Reference yield:

2'-amino-N-(2-bromoethyl)-4'-methoxytosylanilide (86670-79-3) → N1,N1-Diethyl-N3-[(Z)-3-methoxy-10-(toluene-4-sulfonyl)-9,10-dihydro-8H-7-thia-5,10-diaza-benzocycloocten-6-yl]-butane-1,3-diamine; hydrobromide (86670-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / H₂O / 1) 0 deg C, 2 h, 2) 4 deg C, several hours

2: 61 percent / diethyl ether / 3 h / Heating

In diethyl ether; water;

DOI:10.1016/S0040-4020(01)91886-1

upstream raw materials:

N-(4-methoxy-2-nitrophenyl)-4-methylbenzenesulfonamide

N-(2-Bromoethyl)-N-tosyl-4-methoxy-2-nitraniline

2'-amino-N-(2-bromoethyl)-4'-methoxytosylanilide

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