Technology Process of C34H29NO5
There total 8 articles about C34H29NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; tris-(o-tolyl)phosphine; silver carbonate;
In
N,N-dimethyl-formamide;
at 155 ℃;
DOI:10.1016/j.bmcl.2012.09.097
- Guidance literature:
-
Multi-step reaction with 4 steps
1: oxalyl dichloride / dichloromethane / 45 °C
2: triethylamine / dichloromethane / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 20 °C
4: palladium diacetate; tris-(o-tolyl)phosphine; silver carbonate / N,N-dimethyl-formamide / 155 °C
With
oxalyl dichloride; palladium diacetate; sodium hydride; triethylamine; tris-(o-tolyl)phosphine; silver carbonate;
In
dichloromethane; N,N-dimethyl-formamide;
4: |Heck Reaction;
DOI:10.1016/j.bmcl.2012.09.097
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / 90 °C
2: triethylamine / dichloromethane / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 20 °C
4: palladium diacetate; tris-(o-tolyl)phosphine; silver carbonate / N,N-dimethyl-formamide / 155 °C
With
tetrakis(triphenylphosphine) palladium(0); palladium diacetate; sodium hydride; sodium carbonate; triethylamine; tris-(o-tolyl)phosphine; silver carbonate;
In
dichloromethane; water; N,N-dimethyl-formamide; toluene;
4: |Heck Reaction;
DOI:10.1016/j.bmcl.2012.09.097
