2-(6-Chloro-3-pyridinyl)imidodicarbonic acid 1,3-bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:2-(6-Chloro-3-pyridinyl)imidodicarbonic acid 1,3-bis(1,1-dimethylethyl) ester
CAS No.:1044148-99-3
Molecular Formula:C₁₅H₂₁ClN₂O₄
Molecular Weight:328.796
Hs Code.:
Mol file:1044148-99-3.mol

Synonyms:

Suppliers and Price of 2-(6-Chloro-3-pyridinyl)imidodicarbonic acid 1,3-bis(1,1-dimethylethyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-CHloro-5-(N,N-di-boc-amino)pyridine 95+%
5g
$ 1414.00

Crysdot
2-CHloro-5-(N,N-di-boc-amino)pyridine 95+%
1g
$ 460.00

Chemenu
2-CHloro-5-(N,N-di-boc-amino)pyridine 95%
1g
$ 435.00

Chemenu
2-CHloro-5-(N,N-di-boc-amino)pyridine 95%
5g
$ 1332.00

Alichem
2-Chloro-5-(n,n-di-boc-amino)pyridine
5g
$ 1545.00

Alichem
2-Chloro-5-(n,n-di-boc-amino)pyridine
1g
$ 514.50

Total 6 raw suppliers

Chemical Property of 2-(6-Chloro-3-pyridinyl)imidodicarbonic acid 1,3-bis(1,1-dimethylethyl) ester

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

2-CHloro-5-(N,N-di-boc-amino)pyridine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(6-Chloro-3-pyridinyl)imidodicarbonic acid 1,3-bis(1,1-dimethylethyl) ester

There total 1 articles about 2-(6-Chloro-3-pyridinyl)imidodicarbonic acid 1,3-bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5350-93-6
6-Chloro-pyridin-3-ylamine

: 24424-99-5
di-tert-butyl dicarbonate

: 1044148-99-3
3-[di(tert-butoxycarbonyl)amino]-6-chloropyridine

Guidance literature:: In n-heptane; at 20 - 115 ℃;

Reference yield: 71.0%

: 1044148-99-3
3-[di(tert-butoxycarbonyl)amino]-6-chloropyridine

: 171178-45-3
tert-butyl (6-chloropyridin-3-yl)carbamate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃;
DOI:10.1021/jo800854d

Reference yield:

: 1044148-99-3
3-[di(tert-butoxycarbonyl)amino]-6-chloropyridine

: C₂₃H₂₉F₂N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-methyl-pyrrolidin-2-one; iron(III)-acetylacetonate / tetrahydrofuran / 1 h / -30 - 0 °C

2.1: sodium tetrahydroborate / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

2.2: 16 h / 0 - 20 °C

3.1: hydrogenchloride / 1,4-dioxane; water / 2 h / 20 °C

4.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With 1-methyl-pyrrolidin-2-one; hydrogenchloride; sodium tetrahydroborate; iron(III)-acetylacetonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; mineral oil;