C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾
CAS No.:1423693-37-1
Molecular Formula:C₂₇H₂₁N₂O₅*Na
Molecular Weight:476.464
Hs Code.:

C<sub>27</sub>H<sub>21</sub>N<sub>2</sub>O<sub>5</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:

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Chemical Property of C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾

Chemical Property:

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Technology Process of C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾

There total 12 articles about C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 305798-03-2
2-(6-bromonaphthalen-2-yl)acetonitrile

: 1423693-37-1
C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 10 steps

1.1: acetic acid; water; sulfuric acid / 2 h / Reflux

2.1: hydrogenchloride / 2 h / Reflux

3.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

4.1: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

5.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 80 °C / Inert atmosphere

6.1: water; sodium hydroxide / tetrahydrofuran / 1 h / 20 °C

6.2: pH 4

7.1: chloro-trimethyl-silane / 6 h / 20 °C

8.1: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux; Inert atmosphere

9.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C

9.2: pH 3

10.1: sodium hydroxide / water; acetonitrile / 1 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; chloro-trimethyl-silane; sulfuric acid; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; water; acetic acid; triethylamine; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 33626-98-1
methyl 6-bromo-2-naphthoate

: 1423693-37-1
C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 13 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C

2.1: thionyl chloride; zinc(II) chloride / dichloromethane / -5 - 20 °C

3.1: acetonitrile / Reflux

4.1: acetic acid; water; sulfuric acid / 2 h / Reflux

5.1: hydrogenchloride / 2 h / Reflux

6.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

7.1: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

8.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 80 °C / Inert atmosphere

9.1: water; sodium hydroxide / tetrahydrofuran / 1 h / 20 °C

9.2: pH 4

10.1: chloro-trimethyl-silane / 6 h / 20 °C

11.1: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux; Inert atmosphere

12.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C

12.2: pH 3

13.1: sodium hydroxide / water; acetonitrile / 1 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; thionyl chloride; sulfuric acid; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; water; acetic acid; triethylamine; sodium hydroxide; zinc(II) chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 32721-06-5
2-(6-bromonaphthalen-2-yl)acetic acid

: 1423693-37-1
C₂₇H₂₁N₂O₅^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride / 2 h / Reflux

2.1: triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide / N,N-dimethyl-formamide / Inert atmosphere; Reflux

3.1: tetrabutyl ammonium fluoride / dichloromethane / 2 h / 20 °C

4.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 80 °C / Inert atmosphere

5.1: water; sodium hydroxide / tetrahydrofuran / 1 h / 20 °C

5.2: pH 4

6.1: chloro-trimethyl-silane / 6 h / 20 °C

7.1: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux; Inert atmosphere

8.1: lithium hydroxide; water / methanol; tetrahydrofuran / 20 °C

8.2: pH 3

9.1: sodium hydroxide / water; acetonitrile / 1 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; chloro-trimethyl-silane; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; water; triethylamine; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;