Technology Process of C24H39N2O3PS
There total 7 articles about C24H39N2O3PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: thionyl chloride; pyridine / CH2Cl2 / 4 h / 25 °C
2: CH2Cl2 / 18 h / 25 °C
3: toluene
4: tetrahydrofuran / -40 °C
5: trimethyl phosphite; methanol / 60 °C
With
pyridine; methanol; thionyl chloride; phosphorous acid trimethyl ester;
In
tetrahydrofuran; dichloromethane; toluene;
2: Diels-Alder reaction / 3: Staudinger reaction / 6: Dess-Martin oxidation;
DOI:10.1016/S0040-4039(00)01797-4
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: aq. HCl; NaNO2 / 0 °C
1.2: sodium azide; aq. NaOAc
2.1: thionyl chloride; pyridine / CH2Cl2 / 4 h / 25 °C
3.1: CH2Cl2 / 18 h / 25 °C
4.1: toluene
5.1: tetrahydrofuran / -40 °C
6.1: trimethyl phosphite; methanol / 60 °C
With
pyridine; hydrogenchloride; methanol; thionyl chloride; sodium nitrite; phosphorous acid trimethyl ester;
In
tetrahydrofuran; dichloromethane; toluene;
3.1: Diels-Alder reaction / 4.1: Staudinger reaction / 7.1: Dess-Martin oxidation;
DOI:10.1016/S0040-4039(00)01797-4
- Guidance literature:
-
Multi-step reaction with 5 steps
1: CH2Cl2 / 18 h / 25 °C
2: toluene
3: tetrahydrofuran / -40 °C
4: trimethyl phosphite; methanol / 60 °C
With
methanol; phosphorous acid trimethyl ester;
In
tetrahydrofuran; dichloromethane; toluene;
1: Diels-Alder reaction / 2: Staudinger reaction / 5: Dess-Martin oxidation;
DOI:10.1016/S0040-4039(00)01797-4