ruthenocenecarboxaldehyde 4-nitrophenylhydrazone

Base Information

Chemical Name:ruthenocenecarboxaldehyde 4-nitrophenylhydrazone
CAS No.:174409-29-1
Molecular Formula:C₁₇H₁₅N₃O₂Ru
Molecular Weight:394.395
Hs Code.:

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Chemical Property of ruthenocenecarboxaldehyde 4-nitrophenylhydrazone

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Technology Process of ruthenocenecarboxaldehyde 4-nitrophenylhydrazone

There total 1 articles about ruthenocenecarboxaldehyde 4-nitrophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 66507-25-3
ruthenocene carboxylaldheyde

: 100-16-3
4-nitrophenylhydrazone

: 174409-29-1
ruthenocenecarboxaldehyde 4-nitrophenylhydrazone

Guidance literature:: With acetic acid; In ethanol; soln. of Ru complex, NH2NHC6H4NO2 and acetic acid (2 drops) in EtOH heated under reflux for 20 min; cooled to room temp.; filtered; ppt. recrystd. from EtOH; elem. anal.;
DOI:10.1039/b509221c

Reference yield: 16.0%

: 174409-29-1
ruthenocenecarboxaldehyde 4-nitrophenylhydrazone

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 877615-79-7
1'-(4-nitrophenyl)-3'-(ruthenocenyl)pyrazolino[4',5':1,2][60]fullerene

Guidance literature:: With N-bromosuccinimide; triethyl amine; In toluene; under Ar; soln. of NBS and Ru complex in dry CHCl3 stirred at room temp.for 30 min; solvent removed under vac.; soln. of C60 and NEt3 in dry to luene added; stirred at 40°C for 45 min; solvent removed under reduced pressure; flash chromy. (silica gel, toluene); centrifuged with MeOH and Et2O;
DOI:10.1039/b509221c