Technology Process of C40H37N5O2
There total 6 articles about C40H37N5O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
calcium chloride;
In
hexan-1-ol;
at 160 ℃;
for 16h;
DOI:10.1021/ic3020749
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / ethanol / 72 h / 20 °C / 15001.5 Torr
2: calcium chloride / hexan-1-ol / 16 h / 160 °C
With
hydrogen; calcium chloride;
In
ethanol; hexan-1-ol;
DOI:10.1021/ic3020749
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Novozyme 435 / 4 h / 20 °C
2.1: lithium hydroxide monohydrate
3.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
3.2: 1 h / 0 °C
4.1: trimethylsilylazide; tetrabutyl ammonium fluoride / neat (no solvent) / 96 h / 85 °C / Cooling with ice
5.1: hydrogen / ethanol / 72 h / 20 °C / 15001.5 Torr
6.1: calcium chloride / hexan-1-ol / 16 h / 160 °C
With
lithium hydroxide monohydrate; trimethylsilylazide; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; calcium chloride;
In
tetrahydrofuran; ethanol; hexan-1-ol;
DOI:10.1021/ic3020749