EtN(P(OC₆H₃(iPr)2-2,6)2)2

Base Information

Chemical Name:EtN(P(OC₆H₃(iPr)2-2,6)2)2
CAS No.:889678-16-4
Molecular Formula:C₅₀H₇₃NO₄P₂
Molecular Weight:814.081
Hs Code.:

EtN(P(OC<sub>6</sub>H<sub>3</sub>(iPr)2-2,6)2)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of EtN(P(OC₆H₃(iPr)2-2,6)2)2

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Technology Process of EtN(P(OC₆H₃(iPr)2-2,6)2)2

There total 1 articles about EtN(P(OC₆H₃(iPr)2-2,6)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 2078-54-8
2,6-diisopropylphenol

: 17648-17-8
N,N-ethylamin

: 889678-16-4
EtN(P(OC₆H₃(iPr)2-2,6)2)2

Guidance literature:: 2,6-diisopropylphenol; With sodium; In tetrahydrofuran; for 24h; Heating;

N,N-ethylamin; In tetrahydrofuran; for 12h; Heating;
DOI:10.1039/b516316a

Reference yield: 79.0%

: 889678-16-4
EtN(P(OC₆H₃(iPr)2-2,6)2)2

: ammonium hexafluorophosphate

: bis(η3-allyl-μ-chloropalladium(II))

: 947611-48-5
[(EtN(P(OC6H3(iPr)2-2,6)2)2)Pd(η3-allyl)]PF6

Guidance literature:: In acetone; byproducts: NH4Cl; addn. of amine deriv. to soln. of palladium compd. and ammonium salt in dry acetone at room temp., stirring at room emp. for 2 h; filtration, evapn., addn. of acetone, layering with petrol, isolation ofcrystals, elem. anal.;
DOI:10.1039/b703308g

Reference yield: 69.0%

: 889678-16-4
EtN(P(OC₆H₃(iPr)2-2,6)2)2

: bis(η3-allyl-μ-chloropalladium(II))

: 67-64-1
acetone

: 947611-55-4
[(η3-allyl)Pd2Cl(μ-EtN(P(OC6H3(iPr)2-2,6)2)2)]*acetone

Guidance literature:: With K₂CO₃; In acetone; addn. of amine deriv. to suspn. of palladium compd. and K2CO3 in acetoneat room temp., stirring for 6 h; evapn., addn. of distld. acetone, filtration through celite, concn., storage for 24 h, isolation of crystals, elem. anal.;
DOI:10.1039/b703308g