C₁₇H₁₅NO₃S

Base Information

Chemical Name:C₁₇H₁₅NO₃S
CAS No.:1316339-24-8
Molecular Formula:C₁₇H₁₅NO₃S
Molecular Weight:313.377
Hs Code.:

C<sub>17</sub>H<sub>15</sub>NO<sub>3</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₅NO₃S

Chemical Property:

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Technology Process of C₁₇H₁₅NO₃S

There total 9 articles about C₁₇H₁₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 705262-57-3
2-((ethoxycarbonyl)methoxy)-5-iodobenzoic acid methyl ester

: 1316339-24-8
C₁₇H₁₅NO₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium hexamethyldisilazane / toluene / 2 h / 0 - 25 °C

1.2: 1.5 h / 0 - 80 °C

1.3: 2.5 h / 25 - 60 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 15 - 25 °C

3.1: borane-THF / 20 h / 0 - 5 °C

4.1: hydrogenchloride / water / 2 h / 70 °C

5.1: triethylamine

6.1: copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; sodium t-butanolate / N,N-dimethyl-formamide / 15 h / 100 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 0 - 25 °C

8.1: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; copper(l) iodide; borane-THF; 2.9-dimethyl-1,10-phenanthroline; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.1: Claisen condensation / 1.2: Claisen condensation / 1.3: Claisen condensation / 2.1: Horner-Wadsworth-Emmons olefination / 4.1: Pictet-Spengler cyclisation;
DOI:10.1016/j.bmcl.2011.11.050

Reference yield:

: C₁₀H₆INO

: 1316339-24-8
C₁₇H₁₅NO₃S

Guidance literature:: Multi-step reaction with 6 steps

1: borane-THF / 20 h / 0 - 5 °C

2: hydrogenchloride / water / 2 h / 70 °C

3: triethylamine

4: copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; sodium t-butanolate / N,N-dimethyl-formamide / 15 h / 100 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 0 - 25 °C

6: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; copper(l) iodide; borane-THF; 2.9-dimethyl-1,10-phenanthroline; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 2: Pictet-Spengler cyclisation;
DOI:10.1016/j.bmcl.2011.11.050

Reference yield:

: 60770-51-6
5-iodobenzofuran-3(2H)-one

: 1316339-24-8
C₁₇H₁₅NO₃S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydride / tetrahydrofuran / 1 h / 15 - 25 °C

2: borane-THF / 20 h / 0 - 5 °C

3: hydrogenchloride / water / 2 h / 70 °C

4: triethylamine

5: copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; sodium t-butanolate / N,N-dimethyl-formamide / 15 h / 100 °C

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 0 - 25 °C

7: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; copper(l) iodide; borane-THF; 2.9-dimethyl-1,10-phenanthroline; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 1: Horner-Wadsworth-Emmons olefination / 3: Pictet-Spengler cyclisation;
DOI:10.1016/j.bmcl.2011.11.050