{(C₄H₉Sn)2OH(O₂P(C₆H₅)2)3(OSP(C₆H₅)2)2}2*8C₆H₆

Base Information

Chemical Name:{(C₄H₉Sn)2OH(O₂P(C₆H₅)2)3(OSP(C₆H₅)2)2}2*8C₆H₆
CAS No.:116184-77-1
Molecular Formula:8C₆H₆*C₁₃₆H₁₃₈O₁₈P₁₀S₄Sn₄
Molecular Weight:3598.33
Hs Code.:

{(C<sub>4</sub>H<sub>9</sub>Sn)2OH(O<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3(OSP(C<sub>6</sub>H<sub>5</sub>)2)2}2*8C<sub>6</sub>H<sub>6</sub>

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Chemical Property of {(C₄H₉Sn)2OH(O₂P(C₆H₅)2)3(OSP(C₆H₅)2)2}2*8C₆H₆

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Technology Process of {(C₄H₉Sn)2OH(O₂P(C₆H₅)2)3(OSP(C₆H₅)2)2}2*8C₆H₆

There total 1 articles about {(C₄H₉Sn)2OH(O₂P(C₆H₅)2)3(OSP(C₆H₅)2)2}2*8C₆H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.2%

: 2273-43-0
n-butylstannoic acid

: 14278-72-9
diphenylthiophosphinic acid

: 116184-79-3
4Sn⁽⁴⁺⁾*4O^(2-)*4C₄H₉^(1-)*4OP(S)(C₆H₅)2^(1-)={C₄H₉Sn(O)SOP(C₆H₅)2}4

: 116184-77-1
{(C₄H₉Sn)2OH(O₂P(C₆H₅)2)3(OSP(C₆H₅)2)2}2*8C₆H₆

Guidance literature:: In diethyl ether; toluene; byproducts: H2O; mixt. of Sn compd. and diphenylthiophosphinic acid in toluene was heated (azeotropic removal of water) for 4 h, soln. evapd. in vac., to residue was added ether; filtn. of mixt. yielded solid (n-BuSn(O)SOPPh2)4; mother liquor evapd. to dryness, residue was dissolved in CH2Cl2/C6H6 (2:1 vol.), slow evapn. (7 d) yielded ((n-BuSn)2OH(O2PPh2)3(OSPPh2)2)2*8C6H6; elem. anal. for both products;
DOI:10.1021/ja00229a020