C₁₉H₂₆N₂O₆

Base Information

• Chemical Name: C₁₉H₂₆N₂O₆
• CAS No.: 1362735-88-3
• Molecular Formula: C₁₉H₂₆N₂O₆
• Molecular Weight: 378.425
• Mol file: 1362735-88-3.mol

Synonyms:

Chemical Property of C₁₉H₂₆N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₆N₂O₆

There total 4 articles about C₁₉H₂₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxyphenyl ethyl ketene + di-isopropyl azodicarboxylate (2446-83-5) → C19H26N2O6 (1362735-88-3) + C19H26N2O6

Guidance literature:

3-methoxyphenyl ethyl ketene; di-isopropyl azodicarboxylate; In dichloromethane; Inert atmosphere;

With Fe(C(CH)3CNCHCHC(N(CH₂)4))((CCH₃)5); In dichloromethane; at -20 ℃; for 18h; optical yield given as %ee;

DOI:10.1021/ja300799t

Reference yield:

2-(3-methoxyphenyl)butanoic acid (222191-16-4) → C19H26N2O6 (1362735-88-3) + C19H26N2O6

Guidance literature:

Multi-step reaction with 3 steps

1.1: thionyl chloride / dichloromethane / 15 h / 20 °C / Inert atmosphere

2.1: N,N-dimethyl-ethanamine / tetrahydrofuran / 16.17 h / 0 °C / Inert atmosphere

3.1: dichloromethane / Inert atmosphere

3.2: 18 h / -20 °C

With thionyl chloride; N,N-dimethyl-ethanamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja300799t

Reference yield:

C11H13ClO2 (1362736-09-1) → C19H26N2O6 (1362735-88-3) + C19H26N2O6

Guidance literature:

Multi-step reaction with 2 steps

1.1: N,N-dimethyl-ethanamine / tetrahydrofuran / 16.17 h / 0 °C / Inert atmosphere

2.1: dichloromethane / Inert atmosphere

2.2: 18 h / -20 °C

With N,N-dimethyl-ethanamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja300799t

upstream raw materials:

di-isopropyl azodicarboxylate

C₁₁H₁₃ClO₂

m-methoxyphenylacetic acid

2-(3-methoxyphenyl)butanoic acid