Technology Process of cyclo-L-Tyr-L-Tyr
There total 8 articles about cyclo-L-Tyr-L-Tyr which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C24H30N2O7;
With
formic acid;
at 26 ℃;
Inert atmosphere;
In
isopropyl alcohol; toluene;
at 120 ℃;
Inert atmosphere;
DOI:10.1021/jacs.8b10212
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water; 1,4-dioxane / Inert atmosphere
2.1: triethylamine; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 12 h / 0 - 26 °C / Inert atmosphere
3.1: formic acid / 26 °C / Inert atmosphere
3.2: 120 °C / Inert atmosphere
With
formic acid; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide;
In
1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.8b10212
- Guidance literature:
-
Multi-step reaction with 2 steps
1: formic acid; trifluoroacetic acid; water / 2 h / 20 °C
2: butan-1-ol / 2 h / Reflux
With
formic acid; water; trifluoroacetic acid;
In
butan-1-ol;
DOI:10.1074/jbc.M112.443853