Technology Process of C25H23N3O6S
There total 7 articles about C25H23N3O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 1h;
chemoselective reaction;
DOI:10.1002/cmdc.201100194
- Guidance literature:
-
Multi-step reaction with 4 steps
1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
2: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 1 h / 20 °C / Inert atmosphere
3: dichlorotriphenylphosphorane / chloroform / 12 h / 60 °C / Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 1 h / 20 °C
With
lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; caesium carbonate; dichlorotriphenylphosphorane;
In
tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201100194
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetic acid / methanol / 3 h / 45 °C / Molecular sieve; Inert atmosphere
1.2: 12 h / 20 °C / Inert atmosphere
2.1: dichlorotriphenylphosphorane / chloroform / 12 h / 60 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 1 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; acetic acid; dichlorotriphenylphosphorane;
In
tetrahydrofuran; methanol; chloroform;
DOI:10.1002/cmdc.201100194
