tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone)

Base Information

• Chemical Name: tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone)
• CAS No.: 119481-90-2
• Molecular Formula: C₃₂H₃₆N₆O₈S
• Molecular Weight: 664.739

Synonyms:

Chemical Property of tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone)

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Technology Process of tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone)

There total 3 articles about tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) → tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone) (119481-90-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. acetic acid / 4 h

2: Py

With pyridine; In acetic acid;

Reference yield:

D-arabino-[2]hexosulose 2-[(3-amino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone) (110490-19-2) → tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone) (119481-90-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. acetic acid / 4 h

2: Py

With pyridine; In acetic acid;

Reference yield:

acetic anhydride (108-24-7) + D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone) (122147-23-3) → tetra-O-acetyl-aldehydo-keto-D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone) (119481-90-2)

Guidance literature:

With pyridine;

upstream raw materials:

acetic anhydride

D-arabino-[2]hexosulose 2-[(3-benzylideneamino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone)

benzaldehyde

D-arabino-[2]hexosulose 2-[(3-amino-4-methyl-3H-thiazol-2-ylidene)-hydrazone] 1-(methyl-phenyl-hydrazone)

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