C₃₉H₆₁BrO₆

Base Information

Chemical Name:C₃₉H₆₁BrO₆
CAS No.:1307302-44-8
Molecular Formula:C₃₉H₆₁BrO₆
Molecular Weight:705.814
Hs Code.:

C<sub>39</sub>H<sub>61</sub>BrO<sub>6</sub>

Synonyms:

Suppliers and Price of C₃₉H₆₁BrO₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₆₁BrO₆

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₉H₆₁BrO₆

There total 8 articles about C₃₉H₆₁BrO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140710-90-3
25-hydroxy-5E-[6,19,19'-H3]vitamin D3-3β-tert-butyldimethylsilyl ether

: 1307302-44-8
C₃₉H₆₁BrO₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: selenium(IV) oxide / dichloromethane / 0.5 h / Reflux; Inert atmosphere

1.2: 1 h / Reflux; Inert atmosphere

2.1: anthracene; triethylamine / toluene / 1.25 h / UV-irradiation

3.1: pyridinium p-toluenesulfonate / dichloromethane

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran

5.1: dmap; dicyclohexyl-carbodiimide / dichloromethane

With dmap; selenium(IV) oxide; anthracene; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2011.02.025

Reference yield:

: 19356-17-3
calcidiol

: 1307302-44-8
C₃₉H₆₁BrO₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfur dioxide / Reflux

2.1: 1H-imidazole / N,N-dimethyl-formamide

3.1: sodium hydrogencarbonate / ethanol / Reflux

4.1: selenium(IV) oxide / dichloromethane / 0.5 h / Reflux; Inert atmosphere

4.2: 1 h / Reflux; Inert atmosphere

5.1: anthracene; triethylamine / toluene / 1.25 h / UV-irradiation

6.1: pyridinium p-toluenesulfonate / dichloromethane

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane

With 1H-imidazole; dmap; selenium(IV) oxide; anthracene; sulfur dioxide; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2011.02.025

Reference yield:

: 132054-64-9
1α-[((trimethylsilyl)-oxy)]-3β-[((tertiary-butyl-dimethylsilyl)-oxy)], 25-trihydroxy-9,10-5(Z),7(E),10(19)-triene

: 1307302-44-8
C₃₉H₆₁BrO₆

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium p-toluenesulfonate / dichloromethane

2: tetrabutyl ammonium fluoride / tetrahydrofuran

3: dmap; dicyclohexyl-carbodiimide / dichloromethane

With dmap; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2011.02.025