Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)-

Base Information

Chemical Name:Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)-
CAS No.:1297613-75-2
Molecular Formula:C₃₃H₃₁O₄P
Molecular Weight:522.581
Hs Code.:
DSSTox Substance ID:DTXSID401103045
Nikkaji Number:J3.309.076E
Mol file:1297613-75-2.mol

Synonyms:1297613-75-2;1412439-82-7;Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)-;DTXSID401103045;MFCD29905019;MFCD29905020;(11aR)-3,7-Bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin;(11aS)-3,7-Bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin;W19646;Phosphoric acid 6,6'-bis(3,5-dimethylphenyl)-1,1'-spirobiindan-7,7'-diyl ester;1,10-BIS(3,5-DIMETHYLPHENYL)-12-HYDROXY-4,5,6,7-TETRAHYDRODIINDENO[7,1-DE:1',7'-FG][1,3,2]DIOXAPHOSPHOCINE 12-OXIDE;1,10-bis(3,5-dimethylphenyl)-12-hydroxy-4,5,6,7-tetrahydroiindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocine 12-oxide

Suppliers and Price of Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
(11aR)-3,7-Bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, min. 98%
100mg
$ 796.00

Strem Chemicals
(11aR)-3,7-Bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, min. 98%
25mg
$ 234.00

Total 7 raw suppliers

Chemical Property of Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)-

Chemical Property:

Melting Point:235-240 °C
Boiling Point:671.9±65.0 °C(Predicted)
PKA:1.15±0.20(Predicted)
Density:1.34±0.1 g/cm3(Predicted)
XLogP3:8.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:522.19599646
Heavy Atom Count:38
Complexity:846

Purity/Quality:

99%, ^*data from raw suppliers

(11aR)-3,7-Bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-5-oxide-diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, min. 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)C2=C3C4=C(CCC45CCC6=C5C(=C(C=C6)C7=CC(=CC(=C7)C)C)OP(=O)(O3)O)C=C2)C

Technology Process of Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)-

There total 4 articles about Diindeno[7,1-de:1',7'-fg][1,3,2]dioxaphosphocin, 3,7-bis(3,5-dimethylphenyl)-10,11,12,13-tetrahydro-5-hydroxy-, 5-oxide, (11aR)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930784-56-8
(R)-6,6'-di(3,5-dimethylphenyl)-1,1'-spirobiindane-7,7'-diol

: 1297613-75-2,1412439-82-7
C₃₃H₃₁O₄P

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trichlorophosphate / Inert atmosphere

2: hydrogenchloride; water; acetic acid / 1,2-dichloro-ethane / Reflux

With pyridine; hydrogenchloride; water; acetic acid; trichlorophosphate; In 1,2-dichloro-ethane;
DOI:10.1021/jo200302x

Reference yield:

: 1621066-74-7,1807777-59-8
(R)-6,6'-dibromo-2,2',3,3'-tetrahydro-1,1'-spirobis[1H-indole]-7,7'-diphenol

: 1297613-75-2,1412439-82-7
C₃₃H₃₁O₄P

Guidance literature:: Multi-step reaction with 3 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate / 1,4-dioxane; toluene / 105 - 110 °C / Inert atmosphere

2: pyridine; trichlorophosphate / Inert atmosphere

3: hydrogenchloride; water; acetic acid / 1,2-dichloro-ethane / Reflux

With pyridine; hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; water; acetic acid; trichlorophosphate; In 1,4-dioxane; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jo200302x