Technology Process of C74H98N2O4S3
There total 5 articles about C74H98N2O4S3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
piperidine;
In
chloroform;
for 3h;
Inert atmosphere;
Reflux;
DOI:10.1021/ol302738k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / toluene; methanol / 18 h / Inert atmosphere; Reflux
2: sodium tetrahydroborate / dichloromethane; methanol; water / 1 h / 20 °C / Inert atmosphere
3: iodine / 15 h / -20 °C / Inert atmosphere
4: potassium tert-butylate / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere
5: piperidine / chloroform / 3 h / Inert atmosphere; Reflux
With
piperidine; sodium tetrahydroborate; potassium tert-butylate; iodine; potassium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; water; toluene;
DOI:10.1021/ol302738k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / toluene; methanol / 18 h / Inert atmosphere; Reflux
2: sodium tetrahydroborate / dichloromethane; methanol; water / 1 h / 20 °C / Inert atmosphere
3: iodine / 15 h / -20 °C / Inert atmosphere
4: potassium tert-butylate / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere
5: piperidine / chloroform / 3 h / Inert atmosphere; Reflux
With
piperidine; sodium tetrahydroborate; potassium tert-butylate; iodine; potassium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; water; toluene;
DOI:10.1021/ol302738k