C₃₀H₄₁N₅O₂

Base Information

Chemical Name:C₃₀H₄₁N₅O₂
CAS No.:1422268-77-6
Molecular Formula:C₃₀H₄₁N₅O₂
Molecular Weight:503.688
Hs Code.:

C<sub>30</sub>H<sub>41</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₄₁N₅O₂

Chemical Property:

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Technology Process of C₃₀H₄₁N₅O₂

There total 6 articles about C₃₀H₄₁N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422268-75-4
C₃₀H₃₉N₅O₂

: 1422268-77-6
C₃₀H₄₁N₅O₂

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 12h;
DOI:10.1021/jm4000984

Reference yield:

: 35510-04-4
1-bromo-2,4-bis(bromomethyl)benzene

: 1422268-77-6
C₃₀H₄₁N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 0.17 h / 0 °C

2.1: palladium dichloride; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 8 h / 120 °C

3.1: hydroxylamine hydrochloride / ethanol; water / 100 °C

4.1: hydrogen; palladium 10% on activated carbon / methanol / 12 h / 20 °C

With n-butyllithium; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine; palladium dichloride; In tetrahydrofuran; methanol; ethanol; hexane; water; N,N-dimethyl-formamide; 2.1: |Heck Reaction;
DOI:10.1021/jm4000984

Reference yield:

: 1422268-67-4
C₃₄H₃₇BrN₄

: 1422268-77-6
C₃₀H₄₁N₅O₂

Guidance literature:: Multi-step reaction with 3 steps

1: palladium dichloride; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 8 h / 120 °C

2: hydroxylamine hydrochloride / ethanol; water / 100 °C

3: hydrogen; palladium 10% on activated carbon / methanol / 12 h / 20 °C

With palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine; palladium dichloride; In methanol; ethanol; water; N,N-dimethyl-formamide; 1: |Heck Reaction;
DOI:10.1021/jm4000984