C₃₄H₃₆O₆

Base Information

Chemical Name:C₃₄H₃₆O₆
CAS No.:1453218-07-9
Molecular Formula:C₃₄H₃₆O₆
Molecular Weight:540.656
Hs Code.:

C<sub>34</sub>H<sub>36</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₃₆O₆

Chemical Property:

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Technology Process of C₃₄H₃₆O₆

There total 15 articles about C₃₄H₃₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1453218-00-2
(3aR,4aS,5S,8aR,8bR)-5,8a-bis(benzyloxy)-2,2-dimethyl-4a-((naphthalen-2-ylmethoxy)methyl)octahydro[1,3]dioxolo[4,5-b]benzofuran

: 1453218-07-9
C₃₄H₃₆O₆

Guidance literature:: With iron(III) chloride hexahydrate; In dichloromethane; at 0 - 23 ℃; for 1h;
DOI:10.1021/jo401170y

Reference yield:

: 1453217-93-0
(3aR,4aS,5S,8aR,8bR)-5-((tert-butyldimethylsilyl)oxy)-4a-(((tert-butyldiphenylsilyl)oxy)methyl)-8a-hydroxy-2,2-dimethylhexahydro[1,3]dioxolo[4,5-b]benzofuran-7(4aH)-one

: 1453218-07-9
C₃₄H₃₆O₆

Guidance literature:: Multi-step reaction with 8 steps

1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 7 h / 0 - 23 °C / Inert atmosphere

2: dmap / dichloromethane / 19 h / 40 °C / Inert atmosphere

3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.25 h / 110 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 23 °C / Inert atmosphere

7: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; N,N-dimethyl-formamide; tetrahydrofuran / 3 h / 0 - 23 °C / Inert atmosphere

8: iron(III) chloride hexahydrate / dichloromethane / 1 h / 0 - 23 °C

With dmap; 2,2'-azobis(isobutyronitrile); iron(III) chloride hexahydrate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 3: |Barton-McCombie Deoxygenation;
DOI:10.1021/jo401170y

Reference yield:

: 956485-08-8
((3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 1453218-07-9
C₃₄H₃₆O₆

Guidance literature:: Multi-step reaction with 15 steps

1.1: pyridinium chlorochromate / dichloromethane / 13 h / 40 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -41 °C / Inert atmosphere

2.2: 2 h / -41 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 6 h / 23 °C

5.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 18 h / 23 °C / Inert atmosphere

6.1: oxygen; copper diacetate; palladium dichloride / water; N,N-dimethyl acetamide / 24 h / 40 °C

7.1: L-proline / dimethyl sulfoxide / 54 h / 55 °C / Inert atmosphere

8.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 7 h / 0 - 23 °C / Inert atmosphere

9.1: dmap / dichloromethane / 19 h / 40 °C / Inert atmosphere

10.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.25 h / 110 °C

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

12.1: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

13.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 23 °C / Inert atmosphere

14.1: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; N,N-dimethyl-formamide; tetrahydrofuran / 3 h / 0 - 23 °C / Inert atmosphere

15.1: iron(III) chloride hexahydrate / dichloromethane / 1 h / 0 - 23 °C

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); iron(III) chloride hexahydrate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; oxygen; tri-n-butyl-tin hydride; copper diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; palladium dichloride; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 2.1: |Sakurai Allylation / 5.1: |Wacker Oxidation / 7.1: |Aldol Condensation / 10.1: |Barton-McCombie Deoxygenation;
DOI:10.1021/jo401170y