Technology Process of C27H35NO5
There total 8 articles about C27H35NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 0.5 h / 0 °C
2: triethylamine / dichloromethane / 19 h / 0 - 20 °C
With
triethylamine;
In
dichloromethane;
DOI:10.1039/c3cc48818g
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
2.2: 35 h / 20 °C
3.1: acetic acid / water / 5 h
4.1: sodium tetrahydroborate / methanol / 0.15 h / 0 - 20 °C
5.1: triethylamine / dichloromethane / 0.5 h / 0 °C
6.1: sodium azide / N,N-dimethyl-formamide / 3 h / 70 °C
7.1: triphenylphosphine; water / tetrahydrofuran / 31 h / 20 °C / Reflux
8.1: triethylamine / dichloromethane / 19 h / 0 - 20 °C
With
sodium tetrahydroborate; lithium aluminium tetrahydride; sodium azide; water; sodium hydride; acetic acid; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3cc48818g
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetic acid / water / 5 h
2: sodium tetrahydroborate / methanol / 0.15 h / 0 - 20 °C
3: triethylamine / dichloromethane / 0.5 h / 0 °C
4: sodium azide / N,N-dimethyl-formamide / 3 h / 70 °C
5: triphenylphosphine; water / tetrahydrofuran / 31 h / 20 °C / Reflux
6: triethylamine / dichloromethane / 19 h / 0 - 20 °C
With
sodium tetrahydroborate; sodium azide; water; acetic acid; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc48818g