3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

Base Information

Chemical Name:3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine
CAS No.:1295642-40-8
Molecular Formula:C₃₉H₃₂N₄O₂S₂
Molecular Weight:652.841
Hs Code.:

3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

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Chemical Property of 3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

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Technology Process of 3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

There total 3 articles about 3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1295642-40-8
3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

Guidance literature:: Multi-step reaction with 3 steps

3: triethylamine / dichloromethane / 24 h / 20 °C

With triethylamine; In dichloromethane; 2: Michael addition;
DOI:10.1002/jhet.520

Reference yield:

: 1295642-22-6
3-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-1-(4-methoxyphenyl)-2-propen-1-one

: 1295642-40-8
3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

Guidance literature:: Multi-step reaction with 2 steps

2: triethylamine / dichloromethane / 24 h / 20 °C

With triethylamine; In dichloromethane; 1: Michael addition;
DOI:10.1002/jhet.520

Reference yield:

: 24628-83-9
3-methyl-1-phenyl-5-(phenylsulfanyl)-1H-pyrazole-4-carbaldehyde

: 1295642-40-8
3a,4,5,11-tetrahydro-1-phenyl-3a-(4-methoxyphenyl)-5-(3-methyl-1-phenyl-5-phenylthio-1H-pyrazol-4-yl)-[1,2,4]oxadiazolo[5,4-d][1,5]benzothiazepine

Guidance literature:: Multi-step reaction with 3 steps

3: triethylamine / dichloromethane / 24 h / 20 °C

With triethylamine; In dichloromethane; 2: Michael addition;
DOI:10.1002/jhet.520