Technology Process of C55H50NO9P
There total 7 articles about C55H50NO9P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
at 60 ℃;
for 24h;
Inert atmosphere;
Sealed tube;
DOI:10.1002/anie.201100738
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: nickel dichloride / 5 h / 180 °C / Inert atmosphere; Sealed tube
2.1: trimethylsilyl bromide / dichloromethane / 36 h / 20 °C / Inert atmosphere
2.2: 0.5 h / 20 °C
3.1: phosphorus pentachloride / 17 h / 90 °C / Inert atmosphere
4.1: pyridine / 24 h / 60 °C / Inert atmosphere; Sealed tube
With
pyridine; trimethylsilyl bromide; phosphorus pentachloride; nickel dichloride;
In
dichloromethane;
DOI:10.1002/anie.201100738
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 190 °C / Inert atmosphere
1.2: Reflux; Inert atmosphere
2.1: nickel dichloride / 5 h / 180 °C / Inert atmosphere; Sealed tube
3.1: trimethylsilyl bromide / dichloromethane / 36 h / 20 °C / Inert atmosphere
3.2: 0.5 h / 20 °C
4.1: phosphorus pentachloride / 17 h / 90 °C / Inert atmosphere
5.1: pyridine / 24 h / 60 °C / Inert atmosphere; Sealed tube
With
pyridine; trimethylsilyl bromide; phosphorus pentachloride; toluene-4-sulfonic acid; nickel dichloride;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1002/anie.201100738
