C₅₆H₈₈O₇S₂Si₂

Base Information

Chemical Name:C₅₆H₈₈O₇S₂Si₂
CAS No.:1283735-98-7
Molecular Formula:C₅₆H₈₈O₇S₂Si₂
Molecular Weight:993.614
Hs Code.:

C<sub>56</sub>H<sub>88</sub>O<sub>7</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₅₆H₈₈O₇S₂Si₂

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Technology Process of C₅₆H₈₈O₇S₂Si₂

There total 18 articles about C₅₆H₈₈O₇S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1283735-97-6
C₂₇H₄₂O₃Si₂

: 1283735-96-5
C₂₉H₄₆O₄S₂

: 1283735-98-7
C₅₆H₈₈O₇S₂Si₂

: C₅₆H₈₈O₇S₂Si₂

Guidance literature:: C₂₉H₄₆O₄S₂; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

C₂₇H₄₂O₃Si₂; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1002/asia.201000882

Reference yield:

: 1202747-69-0
C₂₁H₃₀O₃Si

: 1283735-98-7
C₅₆H₈₈O₇S₂Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole; dmap / 0 - 20 °C

2.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 6 h / 0 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C

4.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.2: -78 - 20 °C

With 1H-imidazole; dmap; n-butyllithium; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/asia.201000882

Reference yield:

: 1283735-82-9
C₂₂H₃₄O₄

: 1283735-98-7
C₅₆H₈₈O₇S₂Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

3.1: pyridine; dmap / 5 h / 0 °C

4.1: pyridine; methanesulfonyl chloride / 5 h / 0 - 55 °C

5.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); cyclohexane-1,2-epoxide / tetrachloromethane / 10 h / 90 °C

6.1: methanol; potassium carbonate / 20 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 °C

8.1: toluene-4-sulfonic acid / dichloromethane / 4 h / 0 °C

9.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

9.2: -78 - 20 °C

With pyridine; methanol; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; 2,2'-azobis(isobutyronitrile); cyclohexane-1,2-epoxide; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1002/asia.201000882