n-butyl N-benzyloxycarbonylglycinoate

Base Information

Chemical Name:n-butyl N-benzyloxycarbonylglycinoate
CAS No.:174872-57-2
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:

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Chemical Property of n-butyl N-benzyloxycarbonylglycinoate

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Technology Process of n-butyl N-benzyloxycarbonylglycinoate

There total 3 articles about n-butyl N-benzyloxycarbonylglycinoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1212-53-9
methyl N-benzyloxycarbonylglycinate

: 71-36-3
butan-1-ol

: 174872-57-2
n-butyl N-benzyloxycarbonylglycinoate

Guidance literature:: With C₁₂H₆F₁₈O₁₃Zn₄; In di-isopropyl ether; for 18h; Reflux; Inert atmosphere;
DOI:10.1055/s-0031-1290096

Reference yield: 84.0%

: 108849-83-8,10239-27-7
N-(N-benzyloxycarbonyl-glycyl)-L-serine methyl ester

: 71-36-3
butan-1-ol

: 174872-57-2
n-butyl N-benzyloxycarbonylglycinoate

Guidance literature:: With zinc trifluoromethanesulfonate; Diethyl carbonate; for 45h; Inert atmosphere; Reflux; Solvolysis;
DOI:10.1002/anie.201201789

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 174872-57-2
n-butyl N-benzyloxycarbonylglycinoate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / Inert atmosphere

2: zinc trifluoromethanesulfonate; Diethyl carbonate / 45 h / Inert atmosphere; Reflux; Solvolysis

With zinc trifluoromethanesulfonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Diethyl carbonate;
DOI:10.1002/anie.201201789