Technology Process of C52H76N2O4
There total 5 articles about C52H76N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; water; potassium carbonate;
In
ethanol; toluene;
at 80 ℃;
for 10h;
DOI:10.1016/j.cclet.2011.01.032
- Guidance literature:
-
Multi-step reaction with 3 steps
1: iodine; potassium iodide; potassium hydroxide / water / 8 h / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 110 °C
3: tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; water; potassium carbonate / ethanol; toluene / 10 h / 80 °C
With
tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; water; iodine; potassium carbonate; potassium iodide; potassium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.cclet.2011.01.032
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 110 °C
2: boric acid tributyl ester; iodine; magnesium / tetrahydrofuran / 4 h / 40 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; water; potassium carbonate / ethanol; toluene / 10 h / 80 °C
With
tetrakis(triphenylphosphine) palladium(0); boric acid tributyl ester; tetrabutylammomium bromide; water; iodine; potassium carbonate; magnesium;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.cclet.2011.01.032
