Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾

Base Information

Chemical Name:Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾
CAS No.:1426395-37-0
Molecular Formula:Br*C₃₃H₄₈NO₃P₂
Molecular Weight:648.601
Hs Code.:

Br<sup>(1-)</sup>*C<sub>33</sub>H<sub>48</sub>NO<sub>3</sub>P<sub>2</sub><sup>(1+)</sup>

Synonyms:

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Chemical Property of Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾

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Technology Process of Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾

There total 6 articles about Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 1426395-37-0
Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanol / 6 h / 20 °C

2.1: triethylamine / dichloromethane

3.1: sodium iodide / acetonitrile / 48 h / 20 °C

4.1: 1,4-dioxane / 12 h / 80 °C / Darkness

5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C

6.1: triethylamine; magnesium sulfate / dichloromethane / 1 h / 20 °C / pH 6.5 - 7 / Inert atmosphere

6.2: Inert atmosphere

7.1: dichloromethane / 48 h / Inert atmosphere; Reflux

With hydrogenchloride; magnesium sulfate; triethylamine; sodium iodide; In 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm301866e

Reference yield:

: 75937-12-1
6-(Boc-amino)-1-hexanol

: 1426395-37-0
Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane

2.1: sodium iodide / acetonitrile / 48 h / 20 °C

3.1: 1,4-dioxane / 12 h / 80 °C / Darkness

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C

5.1: triethylamine; magnesium sulfate / dichloromethane / 1 h / 20 °C / pH 6.5 - 7 / Inert atmosphere

5.2: Inert atmosphere

6.1: dichloromethane / 48 h / Inert atmosphere; Reflux

With hydrogenchloride; magnesium sulfate; triethylamine; sodium iodide; In 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/jm301866e

Reference yield:

: 172846-36-5
(6-iodohexyl)-carbamic acid 1,1-dimethylethyl ester

: 1426395-37-0
Br^(1-)*C₃₃H₄₈NO₃P₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,4-dioxane / 12 h / 80 °C / Darkness

2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C

3.1: triethylamine; magnesium sulfate / dichloromethane / 1 h / 20 °C / pH 6.5 - 7 / Inert atmosphere

3.2: Inert atmosphere

4.1: dichloromethane / 48 h / Inert atmosphere; Reflux

With hydrogenchloride; magnesium sulfate; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm301866e