C₇₆H₅₂N₄

Base Information

• Chemical Name: C₇₆H₅₂N₄
• CAS No.: 1427279-35-3
• Molecular Formula: C₇₆H₅₂N₄
• Molecular Weight: 1021.28
• Mol file: 1427279-35-3.mol

Synonyms:

Chemical Property of C₇₆H₅₂N₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₆H₅₂N₄

There total 2 articles about C₇₆H₅₂N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2H-benzisoindole (232-66-6) + benzaldehyde (100-52-7) → C76H52N4 (1427279-35-3)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -50 - 20 ℃; for 50h; Inert atmosphere;

DOI:10.1016/j.inoche.2012.11.028

Reference yield:

1-Nitronaphthalene (86-57-7) → C76H52N4 (1427279-35-3)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphazine

2: potassium hydroxide / ethylene glycol / 0.5 h / Reflux; Inert atmosphere

3: boron trifluoride diethyl etherate / dichloromethane / 50 h / -50 - 20 °C / Inert atmosphere

With phosphazine; boron trifluoride diethyl etherate; potassium hydroxide; In dichloromethane; ethylene glycol;

DOI:10.1016/j.inoche.2012.11.028

Reference yield: 70.0%

C76H52N4 (1427279-35-3) + cobalt(II) acetate (71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7) → CoH2TPTNP (1427279-38-6)

Guidance literature:

In N,N-dimethyl-formamide; for 0.5h; Reflux; Inert atmosphere;

DOI:10.1016/j.inoche.2012.11.028

upstream raw materials:

1-Nitronaphthalene

2H-benzisoindole

benzaldehyde

Downstream raw materials:

CoH₂TPTNP