C₂₄H₂₂BrN

Base Information

• Chemical Name: C₂₄H₂₂BrN
• CAS No.: 1346155-02-9
• Molecular Formula: C₂₄H₂₂BrN
• Molecular Weight: 404.349
• Mol file: 1346155-02-9.mol

Synonyms:

Chemical Property of C₂₄H₂₂BrN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₂BrN

There total 3 articles about C₂₄H₂₂BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H18BrN + allyl bromide (106-95-6) → C24H22BrN (1346155-02-9)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 3.5h; Inert atmosphere;

DOI:10.1002/adsc.201100303

Reference yield:

benzaldehyde (100-52-7) → C24H22BrN (1346155-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: zinc(II) chloride / methanol / 1 h

1.2: 6 h

2.1: sodium carbonate / N,N-dimethyl-formamide / 3.5 h / 80 °C / Inert atmosphere

With sodium carbonate; zinc(II) chloride; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/adsc.201100303

Reference yield:

1-phenyl-1-(2-amino-5-bromophenyl)ethylene (189252-18-4) → C24H22BrN (1346155-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: zinc(II) chloride / methanol / 1 h

1.2: 6 h

2.1: sodium carbonate / N,N-dimethyl-formamide / 3.5 h / 80 °C / Inert atmosphere

With sodium carbonate; zinc(II) chloride; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/adsc.201100303

upstream raw materials:

allyl bromide

1-phenyl-1-(2-amino-5-bromophenyl)ethylene

benzaldehyde

Downstream raw materials:

N-benzyl-6-bromo-4-phenyl-2-quinolone