Y₂(H)2(((((CH₃)2CH)2C₆H₃NC(C₆H₅)N)2Si(CH₃)2)2)

Base Information

• Chemical Name: Y₂(H)2(((((CH₃)2CH)2C₆H₃NC(C₆H₅)N)2Si(CH₃)2)2)
• CAS No.: 1235564-37-0
• Molecular Formula: C₈₀H₁₀₂N₈Si₂Y₂
• Molecular Weight: 1409.73
• Mol file: 1235564-37-0.mol

Synonyms:

Chemical Property of Y₂(H)2(((((CH₃)2CH)2C₆H₃NC(C₆H₅)N)2Si(CH₃)2)2)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Y₂(H)2(((((CH₃)2CH)2C₆H₃NC(C₆H₅)N)2Si(CH₃)2)2)

There total 1 articles about Y₂(H)2(((((CH₃)2CH)2C₆H₃NC(C₆H₅)N)2Si(CH₃)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Y2Cl3((((CH3)2CH)2C6H3NC(C6H5)N)2Si(CH3)2)2(1-)*Li(1+)*4C4H8O=(((C40H50N4Si)2)Y2Cl3)(Li(C4H8O)4) + phenylsilane (694-53-1) + trimethylsilylmethyllithium (1822-00-0) → Y2(H)2(((((CH3)2CH)2C6H3NC(C6H5)N)2Si(CH3)2)2) (1235564-37-0)

Guidance literature:

In toluene; std. Schlenk techniques; Li-compd. in toluene added to Y-compd. in toluene at 20°C, stirred for 12 h at 0°C and for 3 h at room temp., filtered, concd., PhSiH3 added at -40°C, stirred for 1 h atroom temp., stored at -20°C; decanted, washed with cold hexane, dried at ambient temp. in vac. for 1 h, elem. anal.;

DOI:10.1002/ejic.200901161

upstream raw materials:

phenylsilane

trimethylsilylmethyllithium