C₁₂H₂₂⁽²⁾HO₃PS

Base Information

Chemical Name:C₁₂H₂₂⁽²⁾HO₃PS
CAS No.:1309466-64-5
Molecular Formula:C₁₂H₂₃O₃PS
Molecular Weight:279.345
Hs Code.:

C<sub>12</sub>H<sub>22</sub><sup>(2)</sup>HO<sub>3</sub>PS

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₂₂⁽²⁾HO₃PS

Chemical Property:

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Technology Process of C₁₂H₂₂⁽²⁾HO₃PS

There total 3 articles about C₁₂H₂₂⁽²⁾HO₃PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆H₉⁽²⁾HS

: 2574-25-6
Diisopropyl chlorophosphate

: 1309466-64-5
C₁₂H₂₂⁽²⁾HO₃PS

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja202954b

Reference yield:

: 1309466-84-9
C₈H₁₁⁽²⁾HOS

: 1309466-64-5
C₁₂H₂₂⁽²⁾HO₃PS

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / 24 h / 20 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

With water; sodium hydride; sodium hydroxide; In tetrahydrofuran; mineral oil;
DOI:10.1021/ja202954b

Reference yield:

: 55282-88-7
1-deuteriocyclohex-2-en-1-ol

: 1309466-64-5
C₁₂H₂₂⁽²⁾HO₃PS

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: water; sodium hydroxide / 24 h / 20 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

With water; sodium hydride; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; mineral oil;
DOI:10.1021/ja202954b