C₂₉H₂₄N₂O₃

Base Information

Chemical Name:C₂₉H₂₄N₂O₃
CAS No.:1395923-02-0
Molecular Formula:C₂₉H₂₄N₂O₃
Molecular Weight:448.521
Hs Code.:

C<sub>29</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₄N₂O₃

Chemical Property:

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Technology Process of C₂₉H₂₄N₂O₃

There total 4 articles about C₂₉H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 354764-68-4
3-methoxy-N-(3-aminophenyl)benzamide

: 3973-54-4
2-chloro-10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-one

: 1395923-02-0
C₂₉H₂₄N₂O₃

Guidance literature:: With palladium diacetate; sodium t-butanolate; XPhos; In toluene; tert-butyl alcohol; at 90 ℃; Inert atmosphere;
DOI:10.1021/jm300951u

Reference yield:

: 3973-45-3
2-(3-chlorophenethyl)benzoic acid

: 1395923-02-0
C₂₉H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: aluminum (III) chloride / dichloromethane / 4 h / 20 °C

3: palladium diacetate; XPhos; sodium t-butanolate / tert-butyl alcohol; toluene / 90 °C / Inert atmosphere

With aluminum (III) chloride; oxalyl dichloride; palladium diacetate; N,N-dimethyl-formamide; sodium t-butanolate; XPhos; In dichloromethane; toluene; tert-butyl alcohol; 2: |Friedel-Crafts Acylation / 3: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm300951u

Reference yield:

: 92428-41-6
2-(3-chlorophenethenyl)benzoic acid

: 1395923-02-0
C₂₉H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: 10% Pd/C; hydrogen / ethyl acetate; acetonitrile / 5 h / 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: aluminum (III) chloride / dichloromethane / 4 h / 20 °C

4: palladium diacetate; XPhos; sodium t-butanolate / tert-butyl alcohol; toluene / 90 °C / Inert atmosphere

With aluminum (III) chloride; oxalyl dichloride; 10% Pd/C; hydrogen; palladium diacetate; N,N-dimethyl-formamide; sodium t-butanolate; XPhos; In dichloromethane; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol; 3: |Friedel-Crafts Acylation / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm300951u