N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide

Base Information

Chemical Name:N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide
CAS No.:1360907-30-7
Molecular Formula:C₂₈H₂₂N₂O₄
Molecular Weight:450.494
Hs Code.:

Synonyms:

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Chemical Property of N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide

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Technology Process of N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide

There total 6 articles about N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111079-44-8
2-trimethylsilylfuro<3,2-b>pyridine

: 1360907-30-7
N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C

2.1: trichlorophosphate / 2 h / 100 °C / Sealed tube

3.1: potassium fluoride; N-iodo-succinimide / acetonitrile / 2 h / 20 - 50 °C / Inert atmosphere

4.1: potassium carbonate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane; water / 1 h / 150 °C / Microwave irradiation

5.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 160 °C / Microwave irradiation

6.1: pyridine / N,N-dimethyl-formamide / 0.08 h / Cooling with ice

6.2: 20 °C

With pyridine; potassium fluoride; N-iodo-succinimide; potassium carbonate; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 4.1: Suzuki Coupling;

Reference yield:

: 1071540-49-2
2-(trimethylsilanyl)furo[3,2-b]pyridine 4-oxide

: 1360907-30-7
N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / 2 h / 100 °C / Sealed tube

2.1: potassium fluoride; N-iodo-succinimide / acetonitrile / 2 h / 20 - 50 °C / Inert atmosphere

3.1: potassium carbonate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane; water / 1 h / 150 °C / Microwave irradiation

4.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 160 °C / Microwave irradiation

5.1: pyridine / N,N-dimethyl-formamide / 0.08 h / Cooling with ice

5.2: 20 °C

With pyridine; potassium fluoride; N-iodo-succinimide; potassium carbonate; caesium carbonate; trichlorophosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; 3.1: Suzuki Coupling;

Reference yield:

: 6602-32-0
2-bromo-pyridin-3-ol

: 1360907-30-7
N-{3-[7-(4-phenoxyphenoxy)furo[3,2-b]pyridin-2-yl]phenyl}propanamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: copper(l) iodide / bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 0.08 h / Inert atmosphere

1.2: 18 h / 500 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C

3.1: trichlorophosphate / 2 h / 100 °C / Sealed tube

4.1: potassium fluoride; N-iodo-succinimide / acetonitrile / 2 h / 20 - 50 °C / Inert atmosphere

5.1: potassium carbonate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane; water / 1 h / 150 °C / Microwave irradiation

6.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 160 °C / Microwave irradiation

7.1: pyridine / N,N-dimethyl-formamide / 0.08 h / Cooling with ice

7.2: 20 °C

With pyridine; potassium fluoride; N-iodo-succinimide; copper(l) iodide; potassium carbonate; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; bis-triphenylphosphine-palladium(II) chloride; palladium diacetate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 5.1: Suzuki Coupling;