Technology Process of C27H21NO6S
There total 3 articles about C27H21NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid / 15 h / Inert atmosphere; Reflux
2.1: sodium hydride / N,N-dimethyl-formamide
2.2: 18 h / 80 °C
3.1: piperidine; benzoic acid / toluene / 5 h / Reflux
With
piperidine; sulfuric acid; sodium hydride; benzoic acid;
In
N,N-dimethyl-formamide; toluene;
3.1: Knoevenagel condensation;
DOI:10.1007/s00044-010-9369-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic anhydride; triethylamine / 6 h / 130 - 140 °C
2.1: sulfuric acid / 15 h / Inert atmosphere; Reflux
3.1: sodium hydride / N,N-dimethyl-formamide
3.2: 18 h / 80 °C
4.1: piperidine; benzoic acid / toluene / 5 h / Reflux
With
piperidine; sulfuric acid; acetic anhydride; sodium hydride; triethylamine; benzoic acid;
In
N,N-dimethyl-formamide; toluene;
1.1: Perkin condensation / 4.1: Knoevenagel condensation;
DOI:10.1007/s00044-010-9369-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic anhydride; triethylamine / 6 h / 130 - 140 °C
2.1: sulfuric acid / 15 h / Inert atmosphere; Reflux
3.1: sodium hydride / N,N-dimethyl-formamide
3.2: 18 h / 80 °C
4.1: piperidine; benzoic acid / toluene / 5 h / Reflux
With
piperidine; sulfuric acid; acetic anhydride; sodium hydride; triethylamine; benzoic acid;
In
N,N-dimethyl-formamide; toluene;
1.1: Perkin condensation / 4.1: Knoevenagel condensation;
DOI:10.1007/s00044-010-9369-3
