2-(4-cyanophenyl)-1,3,2-benzodiazaborole

Base Information

• Chemical Name: 2-(4-cyanophenyl)-1,3,2-benzodiazaborole
• CAS No.: 1435933-07-5
• Molecular Formula: C₁₃H₁₀BN₃
• Molecular Weight: 219.053
• Mol file: 1435933-07-5.mol

Synonyms:

Chemical Property of 2-(4-cyanophenyl)-1,3,2-benzodiazaborole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(4-cyanophenyl)-1,3,2-benzodiazaborole

There total 1 articles about 2-(4-cyanophenyl)-1,3,2-benzodiazaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

1,2-diamino-benzene (95-54-5) + 4-cyanophenylboronic acid (126747-14-6) → 2-(4-cyanophenyl)-1,3,2-benzodiazaborole (1435933-07-5)

Guidance literature:

With zirconia balls; at 50 ℃; for 72h; Inert atmosphere;

DOI:10.1021/jo4006238

Reference yield: 99.0%

2-(4-cyanophenyl)-1,3,2-benzodiazaborole (1435933-07-5) → phenazine-2-carbonitrile (6479-93-2)

Guidance literature:

With silver(l) oxide; In dimethyl sulfoxide; at 80 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1039/d1cc06705b

upstream raw materials:

1,2-diamino-benzene

4-cyanophenylboronic acid

Downstream raw materials:

phenazine-2-carbonitrile