4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester
CAS No.:495417-20-4
Molecular Formula:C₂₈H₂₄N₂O₉S
Molecular Weight:564.573
Hs Code.:

4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of 4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of 4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

There total 2 articles about 4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 122-04-3
4-nitro-benzoyl chloride

: 220645-79-4
p-methylphenyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 495417-20-4
4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With bis(tri-n-butyltin)oxide;
DOI:10.1139/v02-131

Reference yield: 35.0%

: 122-04-3
4-nitro-benzoyl chloride

: 220645-79-4
p-methylphenyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 495417-20-4
4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

: C₃₅H₂₇N₃O₁₂S

Guidance literature:: With pyridine; dmap; In tetrahydrofuran;
DOI:10.1139/v02-131

Reference yield: 42.0%

: 807361-40-6
(2S,3R,4R,5S,6S)-3,4,5-Tris-benzyloxy-2-methyl-6-p-tolylsulfanyl-tetrahydro-pyran

: 495417-20-4
4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester

: 358681-61-5
p-methoxyphenyl (2,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: (2S,4S,5R,6R)-4-Acetoxy-5-acetylamino-2-[(4aR,6S,7R,8S,8aS)-7-(4-oxo-pentanoyloxy)-2-phenyl-6-p-tolylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: C₁₄₀H₁₄₉N₃O₄₄

Guidance literature:: 4-Nitro-benzoic acid (2R,3S,4R,5R,6S)-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3,4-dihydroxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-ylmethyl ester; (2S,4S,5R,6R)-4-Acetoxy-5-acetylamino-2-[(4aR,6S,7R,8S,8aS)-7-(4-oxo-pentanoyloxy)-2-phenyl-6-p-tolylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester; With N-iodo-succinimide; trifluorormethanesulfonic acid; silver trifluoromethanesulfonate;

(2S,3R,4R,5S,6S)-3,4,5-Tris-benzyloxy-2-methyl-6-p-tolylsulfanyl-tetrahydro-pyran; With N-iodo-succinimide; trifluorormethanesulfonic acid; silver trifluoromethanesulfonate;

p-methoxyphenyl (2,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside; With N-iodo-succinimide; trifluorormethanesulfonic acid; silver trifluoromethanesulfonate;
DOI:10.1139/v02-131